Search results for "Purified water"
showing 3 items of 3 documents
On-line trace enrichment for the determination of ethacrynic acid in urine by liquid chromatography and column-switching
1993
Abstract A chromatographic method based on liquid chromatography (LC) using column-switching for the determination of ethacrynic acid in urine samples, is described. The proposed system uses a Hypersil ODS-C18, 30 μm (20 mm × 2.1 mm i.d.) pre-column for the pre-concentration and separation of ethacrynic acid from the biological matrix. Polar urinary compounds are removed by flushing the pre-column with purified water, and the enriched analyte is then switched in back-flush mode onto an HP-LiChrospher RP C18, 5 μm (125 × 4 mm i.d.) analytical column, where it is chromatographed using an acetonitrile-acetate buffer gradient elution. The UV detector was set at 275 nm. The recovery of drug was …
BIOPOLYMERS USED AS EDIBLE COATING TO LIMIT WATER TRANSFER, COLOUR DEGRADATION AND AROMA COMPOUND 2-PENTANONE LOST IN MEXICAN FRUITS
2005
Low preservation of typical fruits in countries with warm weather represents a limitation to export. A recently proposed method to increase shelf-life of fresh guava, is the application of biopolymers as edible coatings. This research involves the use of biopolymers of microbial origin obtained with low cost nutrients, to prepare edible coatings applied on mexican guava and apricot. Dextrans obtained by fermentation with Leuconostoc mesenteroides isolated from a typical mexican beverage named pulque (cactus juice fermented). Dextrans were purified by precipitation with methanol and dispersed in purified water. This procedure was repeated 3 times to eliminate carbohydrates others than dextra…
Complex technological and biological research of solutions for peritoneal dialysis
2018
Objective : The purpose of our work was to conduct technological, analytical, and biological investigations and stability studies of peritoneal dialysis (PD) solutions containing glucose and sodium lactate in single-chamber containers. Methods : Different formulations of PD solutions were prepared and sterilized at a temperature of 121 °C during 15 m. UV-spectrophotometric determination was performed using purified water as a blank. The spectra of the solutions were run in the range of 220 to 400 nm for the identification of an absorption maximum (λ max ) and measuring the absorbance at 228-230 nm and λ max before and after heat sterilization. λ max of the most PD solutions after sterilizat…